National Institute of Technology

CMC Facilities and Services

National Institute of Technology, Calicut
Center for Materials Characterization (CMC)
Sl. No.	Instrument Name	Model & Make	Types of samples to be analyzed	Maximum number of Samples accepted at a Time	Maximum number of days required for analysis	Experiment Details		User Charges Rs. (GST Extra)					Faculty In charge Name/Email/ Contact	Technical Staff Name/Email/ Contact
Sl. No.	Instrument Name	Model & Make	Types of samples to be analyzed	Maximum number of Samples accepted at a Time	Maximum number of days required for analysis	Experiment Details		Internal		External Academic Institutes	National Labs / Govt. R&D labs	PSUs/ Industries	Faculty In charge Name/Email/ Contact	Technical Staff Name/Email/ Contact
1	Powder X-Ray Diffractometer	X'Pert3, PANalytical	Solid, Powder, tdin Films,	No restriction	3 days	Normal scan (upto 20 minutes per sample)		175		400	1200	2000	Dr. Hanas T xrdadmin@nitc.ac.in	Ms. Amala A K xrdadmin@nitc.ac.in +91 495 228 6545
						Slow Scan ( more tdan 20 minutes per sample)		200		600	1800	3000
						Additional charges* for using Grazing incidence Set up		50		200	500	750

2	Confocal Raman Spectrometer/Microscope	LabRam HR Evolution, Horiba	Solid, Liquid, Powder, tdin films	No restriction	3 days	Raman Spectra per sample (30 min)		200		400	600	1200	Dr. Maneesh Chandran crsadmin@nitc.ac.in	Ms. Amala A K crsadmin@nitc.ac.in +91 495 228 6545
						Raman Imaging per Sample (60 min)		600		1200	1800	3600
						Additional Charges

3	Liquid Nitrogen Generator	LN40WC	Liquid Nitrogen	Contact Faculty I/C	Contact Faculty I/C	LN2 per litre		25		40	50	60	Dr. Anuj A Vargeese nmradmin@nitc.ac.in	nmradmin@nitc.ac.in +91 495 228 5344
						Cryocan >25 L (Rental Charges/day) #		20		30	40	50
						Cryocan <25 L (Rental Charges/day) #		15		20	25	30

4	500 MHz Solid/Solution state NMR spectrometer	JNM-ECZ500R/S3, JEOL	Solutions and/ Solid	No restriction	3 to 5 Days
						Internal A^Deuterated solvents provided by user. Internal (B): Deuterated Solvents Not Provided		Internal (A)	Internal (B) - NIT Calicut	External Academic Institutes	National Labs / Govt. R&D labs	PSUs/Industries	Dr. Anuj A Vargeese nmradmin@nitc.ac.in	nmradmin@nitc.ac.in / +91 495 228 5344
						1H NMR (First 10 minutes) + 25 for every additional 15 minutes	CDCl3	50	125	200	375	600
							DMSO-d6	50	350	450	1050	1700
							D2O	50	400	500	1200	2000
							Acetone	50	950	1050	2850	4700
							Acetonitrile	50	1050	1150	3150	5200
							Metdanol	50	1050	1150	3150	5200
						13C and otder nuclei# (First 10 minutes) + 25 for every additional 15 minutes	CDCl3	50	125	200	375	600
							DMSO-d6	50	350	450	1050	1700
							D2O	50	400	500	1200	2000
							Acetone	50	950	1050	2850	4700
							Acetonitrile	50	1050	1150	3150	5200
							Metdanol	50	1150	1250	3450	5750
						DEPT (First 10 minutes) + 25 for every additional 15 minutes	CDCl3	100	150	200	375	600
							DMSO-d6	100	375	450	1050	1700
							D2O	100	425	500	1200	2000
							Acetone	100	975	1050	2850	4700
							Acetonitrile	100	1075	1150	3150	5200
							Metdanol	100	1175	1250	3450	5750
						2D-COSY (First 10 minutes) + 25 for every additional 15 minutes	CDCl3	100	150	200	375	600
							DMSO-d6	100	375	450	1050	1700
							D2O	100	425	500	1200	2000
							Acetone	100	975	1050	2850	4700
							Acetonitrile	100	1075	1150	3150	5200
							Metdanol	100	1175	1250	3450	5750
						2D-NOESY/ROESY (First 10 minutes) + 25 for every additional 15 minutes	CDCl3	100	150	200	375	600
							DMSO-d6	100	375	450	1050	1700
							D2O	100	425	500	1200	2000
							Acetone	100	975	1050	2850	4700
							Acetonitrile	100	1075	1150	3150	5200
							Metdanol	100	1175	1250	3450	5750
						Variable Temp. Experiments (VT charges) + charges for each measurement as above at each temperature	Additional /hr	100	100	200	400	600
						Solid state	1st hr	1000	1000	1500	2500	4000
						Solid state	Additional charges/hr	500	750	1000	1500	2000
						^Deuterated solvents provided by user # 19F, 31P, 27Al, 11B, 77Se, 125Te, 95Mo, 29Si measurements also will be done at same charges • For solid state NMR analysis, sample details must be provided. • If TMS spike is required, additional cost of Rs.50/- to be added. • Sample details such as solubility, stability/degradation possibilities should be disclosed at tde time of submission of tde sample. tde centre will not be responsible for any wrong data obtained due to tde degradation of sample. • Sufficient quantity of tde sample should be made available for analysis. • Analysis and in-deptd interpretation of tde results are not included in tde above charges. • Such services shall be provided on a consultation basis. For furtder details, contact tde Faculty-In-Charge. • All users who wish to avail tde facility need to book tde slot well in advance. • All investigators are expected to acknowledge tde services of tde centre in publications and similar articles.

Thematic Centres